REFINERY SEPARATION PROCESSES - 2020/1

Module code: ENG3199

Module Overview

Multicomponent separation is the most commonly used industrial separation process and a sound understanding of the fundamental principles (material/energy balances, vapour-liquid, liquid-solid, gas-solid and liquid-liquid equilibrium, separation efficiency and system hydrodynamics) defining the operation of such processes is essential to a graduate engineer.  This module extends a students knowledge and understanding to include multicomponent systems involving distillation, ultra-filtration and adsorption.

Module provider

Chemical and Process Engineering

Module Leader

MILLINGTON Clive (Chm Proc Eng)

Number of Credits: 15

ECTS Credits: 7.5

Framework: FHEQ Level 6

JACs code: H850

Module cap (Maximum number of students): N/A

Module Availability

Semester 1

Prerequisites / Co-requisites

Completion of the progression requirements to FHEQ Level 6 of degree courses in Chemical Engineering and Chemical and Petroleum Engineering or equivalent

Module content

Indicative content includes:

Introduction

Yield and Separation Factor

Effect of operating variables on performance

Multicomponent Liquid/Vapour Systems

Ideal Systems           

Definition of K value and use

Dew/bubble point calculations

 

            Non-ideal systems

Cubic equations of state

Fugacity and compressibility

Activity and Gibbs-Duhem equation

Activity models

Azeotropes

Adsorbents and adsorption isotherms

Ideal Single Stage Vapour/Liquid Separation

Adiabatic single stage equilibrium

Isenthalpic single stage equilibrium

Control of "flash" vessels

Multicomponent Distillation

Effect of operational variables on internal flows and product quality

Internal flow rates, concentration and temperature profiles

           Nmin and Rmin

           Key and non-key components

           Shortcut Design Method

Fenske equation

Underwood equatio

Gilliland / Eduljee correlation

Kirkbride correlation

Use of equation set

Plate to plate design

Generalised methods

MESH equations, matrix solutions

Inside out and rigorous solution

Complex Fractionation

Complex petroleum fractionation

TBP curves and pseudo components

           Pump-arounds, side streams, multiple products

           Control of complex fractionation

Column and Stage Efficiency

Basic definitions and correlations

Tray and Column Hydraulics

Hydraulic design and operation

Hydraulic gradient and tray passes

Pressure drop, tray pressure balance and downcomer backup

Froth height and tray spacing

           Design variables and effects on operation

           Hydraulic malfunctions

Fluid/Solid and Bio-separations

Membranes, ultra-filtration, reverse osmosis

           Adsorption column design

Petroleum Separation Processes

Separation/removal of fine catalyst particles from vapour and flue gas streams on the fluid catalytic cracking process involving equipment such as cyclones, electrostatic precipitators and wet gas scrubbers.

Assessment pattern

Assessment type Unit of assessment Weighting
School-timetabled exam/test Class Test 1 (45 minute test on multicomponent equilibrium) 10
School-timetabled exam/test Class Test 2 (45 minute test on multicomponent separation) 10
Examination Examination (2 hours) 80

Alternative Assessment

New examination and class tests.

Assessment Strategy

The assessment strategy is designed to provide students with the opportunity to demonstrate their knowledge and analytical skills over the full range of module material and to encourage progressive learning.

Thus, the summative assessment for this module consists of:


  • Class Tests – 20%, 2x45 minute (10% each test), (LO1, LO3)

  • Examination – 80%, 2 hours (LO1, LO2, LO3, LO4)  



Formative assessment

None

Feedback

Verbal feedback during tutorial sessions and the optional drop-in sessions, written feedback from Class Tests.

Module aims

  • a systematic appreciation and critical awareness of the importance of component separation to the process industry
  • a comprehensive appreciation of the characteristics of the separation of ideal and non-ideal multicomponent systems using a variety of techniques
  • an in-depth appreciation of the inter-relationships between the separation performance and operating parameters of multicomponent separating devices
  • a knowledge of the design methodologies of multicomponent distillation columns
  • an appreciation of the effects of hydraulic malfunction on separation efficiency and the ability to propose feasible scenarios of malfunction based on operating data
  • prepare a scoping design and initial sizing of some separation operations of fluid/solid and biological systems, based on adsorption, and membranes.

Learning outcomes

Attributes Developed
001 Propose suitable models to explain the complexity of multicomponent multiphase equilibrium and to test and confirm their applicability. KC
002 Explain the operating characteristics of multicomponent separating devices and their inter-relationship and analyse the appropriate equilibrium, material and energy balances. KC
003 Confidently scope out a distillation column design in sufficient detail to efficiently set up a process simulator to carry out a design simulation. KCP
004 Accurately prepare a scoping design and initial sizing of some fluid/solid and biological separation operations based on either adsorption or membranes. KC

Attributes Developed

C - Cognitive/analytical

K - Subject knowledge

T - Transferable skills

P - Professional/Practical skills

Overall student workload

Independent Study Hours: 100

Lecture Hours: 44

Tutorial Hours: 6

Methods of Teaching / Learning

The learning and teaching strategy is designed to:


  • Take students logically through the challenging material associated with complex multicomponent multiphase separation.

  • To ensure a logical and progressive learning experience

  • To allow students to practice their skills on a series of real life tutorial problems in a supportive environment.



The learning and teaching methods include:


  • Lectures                                 4 hours per week for 11 weeks (average)

  • Tutorials                                 0.5 hour per week for 12 weeks (average)

  • Class Tests                             2 x 0.75 hours (nominally in weeks 6 and 11)

  • Independent Learning            98.5 hours in total (8.21 hours per week for 12 weeks (average))


Indicated Lecture Hours (which may also include seminars, tutorials, workshops and other contact time) are approximate and may include in-class tests where one or more of these are an assessment on the module. In-class tests are scheduled/organised separately to taught content and will be published on to student personal timetables, where they apply to taken modules, as soon as they are finalised by central administration. This will usually be after the initial publication of the teaching timetable for the relevant semester.

Reading list

Reading list for REFINERY SEPARATION PROCESSES : http://aspire.surrey.ac.uk/modules/eng3199

Programmes this module appears in

Programme Semester Classification Qualifying conditions
Chemical and Petroleum Engineering BEng (Hons) 1 Compulsory A weighted aggregate mark of 40% is required to pass the module
Chemical and Petroleum Engineering MEng 1 Compulsory A weighted aggregate mark of 40% is required to pass the module

Please note that the information detailed within this record is accurate at the time of publishing and may be subject to change. This record contains information for the most up to date version of the programme / module for the 2020/1 academic year.